Information card for entry 4135063

Structure parameters

• Formula: C30 H24 F3 Ge N O2
• Calculated formula: C30 H24 F3 Ge N O2
• Title of publication: Ligand-Controlled Regiodivergent Palladium-Catalyzed Hydrogermylation of Ynamides.
• Authors of publication: Debrauwer, Vincent; Turlik, Aneta; Rummler, Lénaic; Prescimone, Alessandro; Blanchard, Nicolas; Houk, K. N.; Bizet, Vincent
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• Journal volume: 142
• Journal issue: 25
• Pages of publication: 11153 - 11164
• a: 9.2732 ± 0.0004 Å
• b: 10.0269 ± 0.0003 Å
• c: 27.8796 ± 0.001 Å
• α: 90°
• β: 94.522 ± 0.003°
• γ: 90°
• Cell volume: 2584.22 ± 0.16 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.073
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for all reflections: 0.0845
• Weighted residual factors for significantly intense reflections: 0.0782
• Weighted residual factors for all reflections included in the refinement: 0.0764
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0273
• Diffraction radiation wavelength: 1.34143 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No