Information card for entry 4135465

Structure parameters

• Formula: C128.67 H160 F12 N4 O37.33 Rh4 S4
• Calculated formula: C351 H316 F27 N12 O53 Rh12 S9
• Title of publication: Selective Construction of Very Large Stacking-Interaction-Induced Molecular 818 Metalla-knots and Borromean Ring Using Curved Dipyridyl Ligands
• Authors of publication: Zhang, Hai-Ning; Lin, Yue-Jian; Jin, Guo-Xin
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• a: 36.467 ± 0.004 Å
• b: 29.225 ± 0.004 Å
• c: 42.676 ± 0.005 Å
• α: 90°
• β: 102.209 ± 0.005°
• γ: 90°
• Cell volume: 44453 ± 9 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1497
• Residual factor for significantly intense reflections: 0.1015
• Weighted residual factors for significantly intense reflections: 0.299
• Weighted residual factors for all reflections included in the refinement: 0.3446
• Goodness-of-fit parameter for all reflections included in the refinement: 1.107
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No