Information card for entry 4135466

Structure parameters

• Formula: C150 H167 F12 N5 O26 Rh4 S4
• Calculated formula: C273 H266 F21 N10 O41 Rh8 S7
• Title of publication: Selective Construction of Very Large Stacking-Interaction-Induced Molecular 818 Metalla-knots and Borromean Ring Using Curved Dipyridyl Ligands
• Authors of publication: Zhang, Hai-Ning; Lin, Yue-Jian; Jin, Guo-Xin
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2020
• a: 15.8656 ± 0.0007 Å
• b: 18.5301 ± 0.0008 Å
• c: 27.9838 ± 0.0012 Å
• α: 92.145 ± 0.002°
• β: 104.593 ± 0.002°
• γ: 110.192 ± 0.002°
• Cell volume: 7401.9 ± 0.6 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0655
• Residual factor for significantly intense reflections: 0.0573
• Weighted residual factors for significantly intense reflections: 0.1595
• Weighted residual factors for all reflections included in the refinement: 0.1664
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 1.34138 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No