Information card for entry 4300196

Structure parameters

• Formula: C20 H41 F6 N5 O9 Rh S2
• Calculated formula: C20 H41 F6 N5 O9 Rh S2
• Title of publication: Hydrogen Atom and Hydride Transfer in the Reactions of Chromium(IV) and Chromium(V) Complexes with Rhodium Hydrides. Crystal Structure of a Superoxorhodium(III) Product
• Authors of publication: Andreja Bakac; Ilia A. Guzei
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 736 - 740
• a: 9.4257 ± 0.0005 Å
• b: 13.4119 ± 0.0007 Å
• c: 13.614 ± 0.0007 Å
• α: 72.842 ± 0.001°
• β: 82.082 ± 0.001°
• γ: 75.414 ± 0.001°
• Cell volume: 1587.69 ± 0.14 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0641
• Residual factor for significantly intense reflections: 0.0549
• Weighted residual factors for significantly intense reflections: 0.156
• Weighted residual factors for all reflections included in the refinement: 0.1639
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No