Information card for entry 4304012

Structure parameters

• Formula: C40 H76 Li2 N2 O4 Si2
• Calculated formula: C40 H76 Li2 N2 O4 Si2
• Title of publication: Synthesis, Structures, and Kinetics of Mixed-Donor Amido-Amino-Siloxo Ligands from Symmetrical Diamidosilyl Ether Ligands via a Retro-Brook Rearrangement
• Authors of publication: Farzad Haftbaradaran; Angela M. Kuchison; Michael J. Katz; Gabriele Schatte; Daniel B. Leznoff
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 812 - 822
• a: 19.413 ± 0.0002 Å
• b: 12.335 ± 0.0004 Å
• c: 19.052 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4562.2 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0877
• Residual factor for significantly intense reflections: 0.0745
• Weighted residual factors for significantly intense reflections: 0.2067
• Weighted residual factors for all reflections included in the refinement: 0.2186
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No