Information card for entry 4304013

Structure parameters

• Formula: C22 H36 N2 O Si2
• Calculated formula: C22 H36 N2 O Si2
• SMILES: [Si](O[Si](Nc1c(cc(cc1C)C)C)(C)C)(Nc1c(cc(cc1C)C)C)(C)C
• Title of publication: Synthesis, Structures, and Kinetics of Mixed-Donor Amido-Amino-Siloxo Ligands from Symmetrical Diamidosilyl Ether Ligands via a Retro-Brook Rearrangement
• Authors of publication: Farzad Haftbaradaran; Angela M. Kuchison; Michael J. Katz; Gabriele Schatte; Daniel B. Leznoff
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 812 - 822
• a: 18.432 ± 0.0003 Å
• b: 15.894 ± 0.0007 Å
• c: 8.324 ± 0.0008 Å
• α: 90°
• β: 93.129 ± 0.003°
• γ: 90°
• Cell volume: 2434.9 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0759
• Residual factor for significantly intense reflections: 0.0496
• Weighted residual factors for significantly intense reflections: 0.1108
• Weighted residual factors for all reflections included in the refinement: 0.1266
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No