Information card for entry 4304016

Structure parameters

• Formula: C44 H68 Li4 N4 O2 Si4
• Calculated formula: C44 H68 Li4 N4 O2 Si4
• SMILES: [Si]1(C)(C)[O]23[Li]45[N]1(c1c(cc(cc1C)C)C)[Si](C)(C)[N]14(c4c(cc(cc4C)C)C)[Li]46[N]7(c8c(cc(cc8C)C)C)[Si](C)(C)[O]54[Li]72[N]26(c4c(cc(cc4(C)[Li]312)C)C)[Si](C)C
• Title of publication: Synthesis, Structures, and Kinetics of Mixed-Donor Amido-Amino-Siloxo Ligands from Symmetrical Diamidosilyl Ether Ligands via a Retro-Brook Rearrangement
• Authors of publication: Farzad Haftbaradaran; Angela M. Kuchison; Michael J. Katz; Gabriele Schatte; Daniel B. Leznoff
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 812 - 822
• a: 30.595 ± 0.0002 Å
• b: 11.765 ± 0.0002 Å
• c: 13.382 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4816.9 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.064
• Residual factor for significantly intense reflections: 0.0477
• Weighted residual factors for significantly intense reflections: 0.096
• Weighted residual factors for all reflections included in the refinement: 0.1053
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No