Information card for entry 4304017

Structure parameters

• Formula: C52 H84 Li4 N4 O4 Si4
• Calculated formula: C52 H84 Li4 N4 O4 Si4
• Title of publication: Synthesis, Structures, and Kinetics of Mixed-Donor Amido-Amino-Siloxo Ligands from Symmetrical Diamidosilyl Ether Ligands via a Retro-Brook Rearrangement
• Authors of publication: Farzad Haftbaradaran; Angela M. Kuchison; Michael J. Katz; Gabriele Schatte; Daniel B. Leznoff
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 812 - 822
• a: 12.866 ± 0.0004 Å
• b: 13.953 ± 0.0003 Å
• c: 16.92 ± 0.0005 Å
• α: 70.538 ± 0.0018°
• β: 88.726 ± 0.0012°
• γ: 89.56 ± 0.0013°
• Cell volume: 2863.21 ± 0.14 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0963
• Residual factor for significantly intense reflections: 0.063
• Weighted residual factors for significantly intense reflections: 0.1565
• Weighted residual factors for all reflections included in the refinement: 0.1797
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No