Information card for entry 4304018

Structure parameters

• Formula: C56 H92 Li4 N4 O2 Si4
• Calculated formula: C56 H92 Li4 N4 O2 Si4
• SMILES: [Si]1(C)(C)[O]23[Li]4[N]1(c1c(cccc1C(C)C)C(C)C)[Si](C)(C)[N]4(c1c(cccc1C(C)C)C(C)C)[Li]2[O]12[Si](C)(C(C)C)[N]4(c5c(cccc5C(C)C)C(C)C)[Si](C)(C)[N](c5c(cccc5C(C)C)C(C)C)([Li]32)[Li]14
• Title of publication: Synthesis, Structures, and Kinetics of Mixed-Donor Amido-Amino-Siloxo Ligands from Symmetrical Diamidosilyl Ether Ligands via a Retro-Brook Rearrangement
• Authors of publication: Farzad Haftbaradaran; Angela M. Kuchison; Michael J. Katz; Gabriele Schatte; Daniel B. Leznoff
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 812 - 822
• a: 20.354 ± 0.0005 Å
• b: 14.922 ± 0.0004 Å
• c: 24.685 ± 0.0006 Å
• α: 90°
• β: 125.145 ± 0.0015°
• γ: 90°
• Cell volume: 6130.6 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0985
• Residual factor for significantly intense reflections: 0.0534
• Weighted residual factors for significantly intense reflections: 0.1167
• Weighted residual factors for all reflections included in the refinement: 0.1393
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No