Crystallography Open Database

Information card for entry 4304054

Preview

Coordinates	4304054.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C120 H164 B8 F32 N32 O26 Pd8
Calculated formula	C120 H164 B8 F32 N32 O26 Pd8
Title of publication	Self-Assembly, Structures, and Photophysical Properties of 4,4'-Bipyrazolate-Linked Metallo-Macrocycles with Dimetal Clips
Authors of publication	Qing-Fu Sun; Keith Man-Chung Wong; Li-Xia Liu; Hai-Ping Huang; Shu-Yan Yu; Vivian Wing-Wah Yam; Yi-Zhi Li; Yuan-Jiang Pan; Kai-Chao Yu
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	2142 - 2154
a	25.615 ± 0.005 Å
b	33.112 ± 0.007 Å
c	17.229 ± 0.003 Å
α	90°
β	128.04 ± 0.03°
γ	90°
Cell volume	11509 ± 6 Å³
Cell temperature	291 ± 2 K
Ambient diffraction temperature	291 ± 2 K
Number of distinct elements	7
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0922
Residual factor for significantly intense reflections	0.0554
Weighted residual factors for significantly intense reflections	0.0901
Weighted residual factors for all reflections included in the refinement	0.0952
Goodness-of-fit parameter for all reflections included in the refinement	0.997
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4304054.html