Information card for entry 4304055

Structure parameters

• Formula: C104 H108 B8 F32 N32 O14 Pd8
• Calculated formula: C104 H108 B8 F32 N32 O14 Pd8
• Title of publication: Self-Assembly, Structures, and Photophysical Properties of 4,4'-Bipyrazolate-Linked Metallo-Macrocycles with Dimetal Clips
• Authors of publication: Qing-Fu Sun; Keith Man-Chung Wong; Li-Xia Liu; Hai-Ping Huang; Shu-Yan Yu; Vivian Wing-Wah Yam; Yi-Zhi Li; Yuan-Jiang Pan; Kai-Chao Yu
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 2142 - 2154
• a: 13.973 ± 0.003 Å
• b: 16.063 ± 0.003 Å
• c: 19.451 ± 0.004 Å
• α: 111.18 ± 0.03°
• β: 100.82 ± 0.03°
• γ: 91.69 ± 0.03°
• Cell volume: 3975.8 ± 1.7 ų
• Cell temperature: 291 ± 2 K
• Ambient diffraction temperature: 291 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0769
• Residual factor for significantly intense reflections: 0.0566
• Weighted residual factors for significantly intense reflections: 0.1106
• Weighted residual factors for all reflections included in the refinement: 0.1145
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No