Information card for entry 4304400

Structure parameters

• Formula: C128 H132 B2 Cl2 N8 O4 Os2 P4
• Calculated formula: C128 H132 B2 Cl2 N8 O4 Os2 P4
• Title of publication: Ru and Os Complexes Containing a P,N-Donor Heterotopic Ligand: The Effect of Solvent on Stereochemistry
• Authors of publication: Dabb, Serin L.; Messerle, Barbara A.; Smith, Matthew K.; Willis, Anthony C.
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Journal issue: 8
• Pages of publication: 3034 - 3044
• a: 18.4958 ± 0.0001 Å
• b: 30.271 ± 0.0002 Å
• c: 20.4361 ± 0.0002 Å
• α: 90°
• β: 97.2536 ± 0.0004°
• γ: 90°
• Cell volume: 11350.3 ± 0.15 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.0242
• Weighted residual factors for all reflections: 0.0733
• Weighted residual factors for significantly intense reflections: 0.0561
• Weighted residual factors for all reflections included in the refinement: 0.0733
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9562
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No