Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4304401
Preview
Coordinates | 4304401.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | [TcO3Clbipy] |
---|---|
Formula | C10 H8 Cl N2 O3 Tc |
Calculated formula | C10 H8 Cl N2 O3 Tc |
Title of publication | High-Valent Technetium Complexes with the [99TcO3]+ Core from in Situ Prepared Mixed Anhydrides of [99TcO4]- and Their Reactivities |
Authors of publication | Yuji Tooyama; Henrik Braband; Bernhard Spingler; Ulrich Abram; Roger Alberto |
Journal of publication | Inorganic Chemistry |
Year of publication | 2008 |
Journal volume | 47 |
Pages of publication | 257 - 264 |
a | 7.52742 ± 0.00009 Å |
b | 11.73765 ± 0.00011 Å |
c | 12.86694 ± 0.00014 Å |
α | 90° |
β | 96.2859 ± 0.0011° |
γ | 90° |
Cell volume | 1130.01 ± 0.02 Å3 |
Cell temperature | 183 ± 2 K |
Ambient diffraction temperature | 183 ± 2 K |
Number of distinct elements | 6 |
Space group number | 12 |
Hermann-Mauguin space group symbol | I 1 2/m 1 |
Hall space group symbol | -I 2y |
Residual factor for all reflections | 0.0269 |
Residual factor for significantly intense reflections | 0.0236 |
Weighted residual factors for significantly intense reflections | 0.068 |
Weighted residual factors for all reflections included in the refinement | 0.0696 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.1 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4304401.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.