Information card for entry 4304484

Structure parameters

• Formula: C30 H28 N10 Ni O4
• Calculated formula: C30 H28 N10 Ni O4
• Title of publication: Transition Metal Complexes of 3-Cyano- and 3-Nitroformazans
• Authors of publication: Joe B. Gilroy; Brian O. Patrick; Robert McDonald; Robin G. Hicks
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 1287 - 1294
• a: 12.5875 ± 0.0013 Å
• b: 7.4705 ± 0.0009 Å
• c: 16.7066 ± 0.0018 Å
• α: 90°
• β: 103.689 ± 0.004°
• γ: 90°
• Cell volume: 1526.4 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0771
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for significantly intense reflections: 0.0714
• Weighted residual factors for all reflections included in the refinement: 0.0827
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No