Crystallography Open Database

Information card for entry 4304485

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Coordinates	4304485.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40.5 H52 N10 Ni2 O6
Calculated formula	C38 H46 N10 Ni2 O6
Title of publication	Transition Metal Complexes of 3-Cyano- and 3-Nitroformazans
Authors of publication	Joe B. Gilroy; Brian O. Patrick; Robert McDonald; Robin G. Hicks
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	1287 - 1294
a	11.6602 ± 0.0014 Å
b	19.801 ± 0.002 Å
c	19.807 ± 0.002 Å
α	90°
β	92.5918 ± 0.0016°
γ	90°
Cell volume	4568.4 ± 0.9 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0443
Residual factor for significantly intense reflections	0.0372
Weighted residual factors for significantly intense reflections	0.0996
Weighted residual factors for all reflections included in the refinement	0.1035
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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