Information card for entry 4305052

Structure parameters

• Formula: C30 H28 F6 N5 O Os P
• Calculated formula: C30 H28 F6 N5 O Os P
• Title of publication: Easy Access to Bio-Inspired Osmium(II) Complexes through Electrophilic Intramolecular C(sp2)-H Bond Cyclometalation
• Authors of publication: Ricardo Cerón-Camacho; David Morales-Morales; Simon Hernández; Ronan Le Lagadec; Alexander D. Ryabov
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 4988 - 4995
• a: 9.953 ± 0.002 Å
• b: 12.027 ± 0.001 Å
• c: 14.399 ± 0.002 Å
• α: 101.997 ± 0.002°
• β: 90.836 ± 0.001°
• γ: 100.94 ± 0.001°
• Cell volume: 1652.7 ± 0.4 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.0335
• Weighted residual factors for significantly intense reflections: 0.0685
• Weighted residual factors for all reflections included in the refinement: 0.0704
• Goodness-of-fit parameter for all reflections included in the refinement: 0.897
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No