Crystallography Open Database

Information card for entry 4305053

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Coordinates	4305053.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H26 F6 N5 Os P
Calculated formula	C25 H26 F6 N5 Os P
Title of publication	Easy Access to Bio-Inspired Osmium(II) Complexes through Electrophilic Intramolecular C(sp2)-H Bond Cyclometalation
Authors of publication	Ricardo Cerón-Camacho; David Morales-Morales; Simon Hernández; Ronan Le Lagadec; Alexander D. Ryabov
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	4988 - 4995
a	11.2693 ± 0.0007 Å
b	12.4643 ± 0.0008 Å
c	18.8585 ± 0.0012 Å
α	90°
β	96.271 ± 0.001°
γ	90°
Cell volume	2633.1 ± 0.3 Å³
Cell temperature	291 ± 2 K
Ambient diffraction temperature	291 ± 2 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0356
Residual factor for significantly intense reflections	0.0278
Weighted residual factors for significantly intense reflections	0.0518
Weighted residual factors for all reflections included in the refinement	0.0534
Goodness-of-fit parameter for all reflections included in the refinement	0.88
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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