Synthesis and Structures of Selected Triazapentadienate of Li, Mn, Fe, Co, Ni, Cu(I), and Cu(II) using 2,4-N,N'-Disubstituted 1,3,5-Triazapentadienate Anions as Ancillary Ligands: [N(Ar)C(NMe2)NC(NMe2)N(R)]- (Ar = Ph, 2,6-iPr2-C6H3; R = H, SiMe3)
Authors of publication
Meisu Zhou; Yanping Song; Tao Gong; Hongbo Tong; Jianping Guo; Linhong Weng; Diansheng Liu
Journal of publication
Inorganic Chemistry
Year of publication
2008
Journal volume
47
Pages of publication
6692 - 6700
a
6.1011 ± 0.0015 Å
b
9.633 ± 0.002 Å
c
11.585 ± 0.003 Å
α
81.911 ± 0.003°
β
78.156 ± 0.003°
γ
75.471 ± 0.003°
Cell volume
642.2 ± 0.3 Å3
Cell temperature
298 ± 2 K
Ambient diffraction temperature
298 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.068
Residual factor for significantly intense reflections
0.0636
Weighted residual factors for significantly intense reflections
0.1324
Weighted residual factors for all reflections included in the refinement
0.1346
Goodness-of-fit parameter for all reflections included in the refinement
