Synthesis and Structures of Selected Triazapentadienate of Li, Mn, Fe, Co, Ni, Cu(I), and Cu(II) using 2,4-N,N'-Disubstituted 1,3,5-Triazapentadienate Anions as Ancillary Ligands: [N(Ar)C(NMe2)NC(NMe2)N(R)]- (Ar = Ph, 2,6-iPr2-C6H3; R = H, SiMe3)
Authors of publication
Meisu Zhou; Yanping Song; Tao Gong; Hongbo Tong; Jianping Guo; Linhong Weng; Diansheng Liu
Journal of publication
Inorganic Chemistry
Year of publication
2008
Journal volume
47
Pages of publication
6692 - 6700
a
9.7388 ± 0.0014 Å
b
13.984 ± 0.002 Å
c
16.228 ± 0.002 Å
α
94.386 ± 0.002°
β
96.268 ± 0.002°
γ
102.157 ± 0.002°
Cell volume
2136.3 ± 0.5 Å3
Cell temperature
213 ± 2 K
Ambient diffraction temperature
213 ± 2 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0651
Residual factor for significantly intense reflections
0.0559
Weighted residual factors for significantly intense reflections
0.1583
Weighted residual factors for all reflections included in the refinement
0.1666
Goodness-of-fit parameter for all reflections included in the refinement
