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Information card for entry 4306108
Preview
Coordinates | 4306108.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H57 N2 Ni P2 Si2 |
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Calculated formula | C28 H57 N2 Ni P2 Si2 |
SMILES | [Ni]12[P](C[Si](N1[Si](C)(C)CP(=[N]2c1ccccc1)(C(C)(C)C)C(C)(C)C)(C)C)(C(C)(C)C)C(C)(C)C |
Title of publication | Influence of the Metal Orbital Occupancy and Principal Quantum Number on Organoazide (RN3) Conversion to Transition-Metal Imide Complexes |
Authors of publication | Amy N. Walstrom; Benjamin C. Fullmer; Hongjun Fan; Maren Pink; Drew T. Buschhorn; Kenneth G. Caulton |
Journal of publication | Inorganic Chemistry |
Year of publication | 2008 |
Journal volume | 47 |
Pages of publication | 9002 - 9009 |
a | 10.3244 ± 0.0003 Å |
b | 11.4269 ± 0.0004 Å |
c | 15.5938 ± 0.0005 Å |
α | 106.946 ± 0.0008° |
β | 95.3232 ± 0.0009° |
γ | 106.675 ± 0.0008° |
Cell volume | 1654.27 ± 0.09 Å3 |
Cell temperature | 130 ± 2 K |
Ambient diffraction temperature | 130 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0437 |
Residual factor for significantly intense reflections | 0.0316 |
Weighted residual factors for significantly intense reflections | 0.0788 |
Weighted residual factors for all reflections included in the refinement | 0.0856 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.02 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4306108.html
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