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Information card for entry 4306109
Preview
Coordinates | 4306109.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H57 Cl Fe N4 P2 Si2 |
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Calculated formula | C28 H57 Cl Fe N4 P2 Si2 |
Title of publication | Influence of the Metal Orbital Occupancy and Principal Quantum Number on Organoazide (RN3) Conversion to Transition-Metal Imide Complexes |
Authors of publication | Amy N. Walstrom; Benjamin C. Fullmer; Hongjun Fan; Maren Pink; Drew T. Buschhorn; Kenneth G. Caulton |
Journal of publication | Inorganic Chemistry |
Year of publication | 2008 |
Journal volume | 47 |
Pages of publication | 9002 - 9009 |
a | 10.3791 ± 0.0011 Å |
b | 19.769 ± 0.002 Å |
c | 20.381 ± 0.002 Å |
α | 62.619 ± 0.002° |
β | 79.132 ± 0.003° |
γ | 76.79 ± 0.003° |
Cell volume | 3598.2 ± 0.6 Å3 |
Cell temperature | 130 ± 2 K |
Ambient diffraction temperature | 130 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0553 |
Residual factor for significantly intense reflections | 0.0363 |
Weighted residual factors for significantly intense reflections | 0.0845 |
Weighted residual factors for all reflections included in the refinement | 0.0955 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.006 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4306109.html
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