Information card for entry 4306618

Structure parameters

• Common name: {[Me3NN]Ni}2(mu-OCy)2_cmpd2
• Formula: C58 H80 N4 Ni2 O2
• Calculated formula: C58 H80 N4 Ni2 O2
• Title of publication: Reductive Cleavage of O-, S-, and N-Organonitroso Compounds by Nickel(I) β-Diketiminates
• Authors of publication: Marie M. Melzer; Sarah Jarchow-Choy; Elzbieta Kogut; Timothy H. Warren
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 10187 - 10189
• a: 13.0521 ± 0.0012 Å
• b: 19.2644 ± 0.0017 Å
• c: 20.7729 ± 0.0019 Å
• α: 90°
• β: 95.515 ± 0.001°
• γ: 90°
• Cell volume: 5199 ± 0.8 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.093
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for significantly intense reflections: 0.1362
• Weighted residual factors for all reflections included in the refinement: 0.1527
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No