Crystallography Open Database

Information card for entry 4307546

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Coordinates	4307546.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69 H52.5 Ge6 O8.25 Os4
Calculated formula	C69 H52.5 Ge6 O8.25 Os4
Title of publication	Multiple Additions of Phenylgermanium Ligands to Tetraruthenium and Tetraosmium Carbonyl Cluster Complexes
Authors of publication	Richard D. Adams; Erin M. Boswell; Burjor Captain; Mitul A. Patel
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	533 - 540
a	15.79 ± 0.0006 Å
b	17.9143 ± 0.0007 Å
c	25.2968 ± 0.001 Å
α	90°
β	91.869 ± 0.001°
γ	90°
Cell volume	7151.8 ± 0.5 Å³
Cell temperature	294 ± 2 K
Ambient diffraction temperature	294 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0474
Residual factor for significantly intense reflections	0.0309
Weighted residual factors for significantly intense reflections	0.0855
Weighted residual factors for all reflections included in the refinement	0.0981
Goodness-of-fit parameter for all reflections included in the refinement	1.114
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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