Information card for entry 4307545

Structure parameters

• Formula: C64 H48 Ge5 O9 Os4
• Calculated formula: C64 H48 Ge5 O9 Os4
• SMILES: [Os]12345([Os]678([Os]9%10%11([Os]1([Ge]269c1ccccc1)([Ge]37%10c1ccccc1)([Ge]5(c1ccccc1)c1ccccc1)(C%11=O)(C#[O])C#[O])([Ge]8(c1ccccc1)c1ccccc1)(C#[O])C#[O])([Ge]4(c1ccccc1)c1ccccc1)(C#[O])C#[O])(C#[O])C#[O].c1cc(ccc1)C
• Title of publication: Multiple Additions of Phenylgermanium Ligands to Tetraruthenium and Tetraosmium Carbonyl Cluster Complexes
• Authors of publication: Richard D. Adams; Erin M. Boswell; Burjor Captain; Mitul A. Patel
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 533 - 540
• a: 14.1902 ± 0.0006 Å
• b: 17.1633 ± 0.0007 Å
• c: 18.0443 ± 0.0007 Å
• α: 104.846 ± 0.001°
• β: 106.665 ± 0.001°
• γ: 112.665 ± 0.001°
• Cell volume: 3534.9 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.034
• Residual factor for significantly intense reflections: 0.0288
• Weighted residual factors for significantly intense reflections: 0.0939
• Weighted residual factors for all reflections included in the refinement: 0.0968
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No