Information card for entry 4308328

Structure parameters

• Formula: C46 H96 K3.5 N0.5 O63.5 Si V2 W10
• Calculated formula: C46 K3.5 N0.5 O63.5 Si V2 W10
• Title of publication: Sterically Controlled Esterification on Bis(μ-hydroxo) Dioxovanadium Site in γ-H2SiV2W10O404-
• Authors of publication: Yoshinao Nakagawa; Kazuhiro Uehara; Noritaka Mizuno
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 14 - 16
• a: 15.107 ± 0.007 Å
• b: 17.44 ± 0.008 Å
• c: 21.742 ± 0.012 Å
• α: 81.44 ± 0.02°
• β: 84.21 ± 0.02°
• γ: 67.64 ± 0.02°
• Cell volume: 5232 ± 5 ų
• Cell temperature: 183.1 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.064
• Weighted residual factors for all reflections included in the refinement: 0.073
• Goodness-of-fit parameter for all reflections included in the refinement: 4.079
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No