Crystallography Open Database

Information card for entry 4308769

Preview

Coordinates	4308769.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C45 H43 F6 N3 O P3 Rh
Calculated formula	C45 H43 F6 N3 O P3 Rh
Title of publication	Interactions of Rh(III)-Dihydrido-Bis(phosphine) Complexes with Semicarbazones
Authors of publication	Maria B. Ezhova; Brian O. Patrick; Kapila N. Sereviratne; Brian R. James; Francis J. Waller; Michael E. Ford
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	1482 - 1491
a	12.989 ± 0.0003 Å
b	14.195 ± 0.0005 Å
c	14.7319 ± 0.001 Å
α	67.437 ± 0.002°
β	77.667 ± 0.002°
γ	70.973 ± 0.003°
Cell volume	2359.1 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0657
Residual factor for significantly intense reflections	0.0463
Weighted residual factors for significantly intense reflections	0.1166
Weighted residual factors for all reflections included in the refinement	0.1242
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4308769.html