Information card for entry 4308770

Structure parameters

• Formula: C48 H49 Cl4 F6 N3 O P3 Rh
• Calculated formula: C48 H49 Cl4 F6 N3 O P3 Rh
• Title of publication: Interactions of Rh(III)-Dihydrido-Bis(phosphine) Complexes with Semicarbazones
• Authors of publication: Maria B. Ezhova; Brian O. Patrick; Kapila N. Sereviratne; Brian R. James; Francis J. Waller; Michael E. Ford
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 1482 - 1491
• a: 12.7688 ± 0.0006 Å
• b: 14.4322 ± 0.0008 Å
• c: 14.842 ± 0.001 Å
• α: 97.986 ± 0.002°
• β: 104.637 ± 0.001°
• γ: 98.751 ± 0.002°
• Cell volume: 2570.2 ± 0.3 ų
• Cell temperature: 198.2 K
• Ambient diffraction temperature: 198.2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0666
• Residual factor for significantly intense reflections: 0.039
• Weighted residual factors for all reflections: 0.109
• Weighted residual factors for all reflections included in the refinement: 0.109
• Goodness-of-fit parameter for all reflections: 1.262
• Goodness-of-fit parameter for all reflections included in the refinement: 1.262
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No