Information card for entry 4309380

Structure parameters

• Formula: C34 H74 Al2 N6 P2 Si2
• Calculated formula: C33.991 H74 Al2 N6 P2 Si2
• Title of publication: Synthesis and Structures of Aluminum and Magnesium Complexes of Tetraimidophosphates and Trisamidothiophosphates: EPR and DFT Investigations of the Persistent Neutral Radicals {Me2Al[(μ-NR)(μ-NtBu)P(μ-NtBu)2]Li(THF)2}. (R = SiMe3,tBu)
• Authors of publication: Andrea Armstrong; Tristram Chivers; Heikki M. Tuononen; Masood Parvez
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 5778 - 5788
• a: 20.4 ± 0.006 Å
• b: 16.813 ± 0.004 Å
• c: 12.865 ± 0.011 Å
• α: 90°
• β: 92.31 ± 0.03°
• γ: 90°
• Cell volume: 4409 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0624
• Residual factor for significantly intense reflections: 0.0441
• Weighted residual factors for significantly intense reflections: 0.1071
• Weighted residual factors for all reflections included in the refinement: 0.1193
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No