Information card for entry 4309381

Structure parameters

• Formula: C25 H59 Al Li N4 O2 P Si
• Calculated formula: C24 H59 Al Li N4 O2 P Si1.42
• Title of publication: Synthesis and Structures of Aluminum and Magnesium Complexes of Tetraimidophosphates and Trisamidothiophosphates: EPR and DFT Investigations of the Persistent Neutral Radicals {Me2Al[(μ-NR)(μ-NtBu)P(μ-NtBu)2]Li(THF)2}. (R = SiMe3,tBu)
• Authors of publication: Andrea Armstrong; Tristram Chivers; Heikki M. Tuononen; Masood Parvez
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 5778 - 5788
• a: 10.222 ± 0.002 Å
• b: 17.632 ± 0.004 Å
• c: 18.982 ± 0.004 Å
• α: 90°
• β: 91.152 ± 0.012°
• γ: 90°
• Cell volume: 3420.5 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1644
• Residual factor for significantly intense reflections: 0.0795
• Weighted residual factors for significantly intense reflections: 0.2089
• Weighted residual factors for all reflections included in the refinement: 0.2749
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No