Crystallography Open Database

Information card for entry 4309730

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Coordinates	4309730.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C174 H256 Rh16 S19.22
Calculated formula	C174 H256 Rh16 S19.232
Title of publication	Chemistry of Transition-Metal Clusters with Mixed Sb/S Ligands: Evidence for a Terminal SbS Double Bond in Cp3Rh3Sb2S5 (Cp = C5Me5)
Authors of publication	Andreas Lange; Marek M. Kubicki; Joachim Wachter; Manfred Zabel
Journal of publication	Inorganic Chemistry
Year of publication	2005
Journal volume	44
Pages of publication	7328 - 7332
a	11.3831 ± 0.0007 Å
b	17.0652 ± 0.0014 Å
c	24.2939 ± 0.0016 Å
α	90°
β	100.017 ± 0.008°
γ	90°
Cell volume	4647.3 ± 0.6 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 ± 1 K
Number of distinct elements	4
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0722
Residual factor for significantly intense reflections	0.0449
Weighted residual factors for significantly intense reflections	0.098
Weighted residual factors for all reflections included in the refinement	0.1054
Goodness-of-fit parameter for all reflections included in the refinement	0.924
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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