Information card for entry 4309731

Structure parameters

• Formula: C34 H53 O Rh3 S5 Sb2
• Calculated formula: C34 H53 O Rh3 S5 Sb2
• Title of publication: Chemistry of Transition-Metal Clusters with Mixed Sb/S Ligands: Evidence for a Terminal SbS Double Bond in Cp*3Rh3Sb2S5 (Cp* = C5Me5)
• Authors of publication: Andreas Lange; Marek M. Kubicki; Joachim Wachter; Manfred Zabel
• Journal of publication: Inorganic Chemistry
• Year of publication: 2005
• Journal volume: 44
• Pages of publication: 7328 - 7332
• a: 10.0804 ± 0.0005 Å
• b: 18.5111 ± 0.001 Å
• c: 21.9383 ± 0.0011 Å
• α: 90°
• β: 95.435 ± 0.006°
• γ: 90°
• Cell volume: 4075.3 ± 0.4 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.039
• Residual factor for significantly intense reflections: 0.0271
• Weighted residual factors for significantly intense reflections: 0.0594
• Weighted residual factors for all reflections included in the refinement: 0.0615
• Goodness-of-fit parameter for all reflections included in the refinement: 0.919
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No