Information card for entry 4310598

Structure parameters

• Formula: C54 H52 Ag2 B2 F8 P4
• Calculated formula: C54 H52 Ag2 B2 F8 P4
• Title of publication: Organometallic Oligomers Based on 1,8-Diisocyano-p-menthane (dmb): Syntheses and Characterization of the {[M(diphos)(dmb)]BF4}n and {[Pd2(diphos)2(dmb)](ClO4)2}n Materials (M = Cu, Ag; diphos = dppe, dppp)
• Authors of publication: Eric Fournier; Stéphanie Sicard; Andreas Decken; Pierre D. Harvey
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 1491 - 1501
• a: 10.611 ± 0.0006 Å
• b: 11.3248 ± 0.0007 Å
• c: 12.8341 ± 0.0007 Å
• α: 90.948 ± 0.001°
• β: 114.124 ± 0.001°
• γ: 112.647 ± 0.001°
• Cell volume: 1271.02 ± 0.13 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0271
• Residual factor for significantly intense reflections: 0.0258
• Weighted residual factors for significantly intense reflections: 0.0681
• Weighted residual factors for all reflections included in the refinement: 0.0689
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No