Information card for entry 4310599

Structure parameters

• Formula: C36 H42 Ag B F4 N2 P2
• Calculated formula: C35.97 H33 Ag B F4 N2 P2
• Title of publication: Organometallic Oligomers Based on 1,8-Diisocyano-p-menthane (dmb): Syntheses and Characterization of the {[M(diphos)(dmb)]BF4}n and {[Pd2(diphos)2(dmb)](ClO4)2}n Materials (M = Cu, Ag; diphos = dppe, dppp)
• Authors of publication: Eric Fournier; Stéphanie Sicard; Andreas Decken; Pierre D. Harvey
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 1491 - 1501
• a: 14.113 ± 0.0008 Å
• b: 10.2075 ± 0.0006 Å
• c: 25.8175 ± 0.0016 Å
• α: 90°
• β: 103.381 ± 0.001°
• γ: 90°
• Cell volume: 3618.3 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0324
• Residual factor for significantly intense reflections: 0.0292
• Weighted residual factors for significantly intense reflections: 0.0828
• Weighted residual factors for all reflections included in the refinement: 0.0845
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No