Information card for entry 4310600

Structure parameters

• Formula: C37 H44 B Cu F4 N2 P2
• Calculated formula: C37 H41.3 B Cu F4 N2 P2
• Title of publication: Organometallic Oligomers Based on 1,8-Diisocyano-p-menthane (dmb): Syntheses and Characterization of the {[M(diphos)(dmb)]BF4}n and {[Pd2(diphos)2(dmb)](ClO4)2}n Materials (M = Cu, Ag; diphos = dppe, dppp)
• Authors of publication: Eric Fournier; Stéphanie Sicard; Andreas Decken; Pierre D. Harvey
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 1491 - 1501
• a: 15.5433 ± 0.0009 Å
• b: 11.2094 ± 0.0006 Å
• c: 21.4362 ± 0.0012 Å
• α: 90°
• β: 92.483 ± 0.001°
• γ: 90°
• Cell volume: 3731.3 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0458
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for significantly intense reflections: 0.0905
• Weighted residual factors for all reflections included in the refinement: 0.0976
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No