Information card for entry 4311512

Structure parameters

• Formula: C26 H27 F P Rh
• Calculated formula: C26 H27 F P Rh
• SMILES: [Rh]123([P](c4ccccc4)(c4ccccc4)c4ccccc4)(F)[CH]4=[CH]1CC[CH]2=[CH]3CC4
• Title of publication: Synthesis and Reactivity of Fluoro Complexes: Part 2.1 Rhodium(I) Fluoro Complexes with Alkene and Phosphine Ligands. Synthesis of the First Isolated Rhodium(I) Bifluoride Complexes. Structure of [Rh3(μ3-OH)2(COD)3](HF2) by X-ray Powder Diffraction
• Authors of publication: José Vicente; Juan Gil-Rubio; Delia Bautista; Angelo Sironi; Norberto Masciocchi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 5665 - 5675
• a: 12.7652 ± 0.0007 Å
• b: 11.3795 ± 0.0007 Å
• c: 14.6419 ± 0.0008 Å
• α: 90°
• β: 95.728 ± 0.004°
• γ: 90°
• Cell volume: 2116.3 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0244
• Residual factor for significantly intense reflections: 0.0205
• Weighted residual factors for all reflections: 0.0498
• Weighted residual factors for significantly intense reflections: 0.049
• Goodness-of-fit parameter for all reflections: 1.057
• Goodness-of-fit parameter for significantly intense reflections: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No