Information card for entry 4311513

Structure parameters

• Formula: C26 H28 F2 P Rh
• Calculated formula: C26 H27 F2 P Rh
• Title of publication: Synthesis and Reactivity of Fluoro Complexes: Part 2.1 Rhodium(I) Fluoro Complexes with Alkene and Phosphine Ligands. Synthesis of the First Isolated Rhodium(I) Bifluoride Complexes. Structure of [Rh3(μ3-OH)2(COD)3](HF2) by X-ray Powder Diffraction
• Authors of publication: José Vicente; Juan Gil-Rubio; Delia Bautista; Angelo Sironi; Norberto Masciocchi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2004
• Journal volume: 43
• Pages of publication: 5665 - 5675
• a: 13.8193 ± 0.0014 Å
• b: 11.0201 ± 0.0014 Å
• c: 15.018 ± 0.002 Å
• α: 90°
• β: 101.083 ± 0.005°
• γ: 90°
• Cell volume: 2244.4 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0339
• Weighted residual factors for all reflections: 0.0836
• Weighted residual factors for significantly intense reflections: 0.0708
• Goodness-of-fit parameter for all reflections: 1.009
• Goodness-of-fit parameter for significantly intense reflections: 1.083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No