Information card for entry 4312423

Structure parameters

• Formula: C24 H66 Ge N2 P2 Pd S Si4
• Calculated formula: C24 H66 Ge N2 P2 Pd S Si4
• Title of publication: Reactions of Palladium Germylene Complexes: Formation of Sulfide Bridges
• Authors of publication: Zuzanna T. Cygan; Jeff W. Kampf; Mark M. Banaszak Holl
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7219 - 7226
• a: 16.064 ± 0.003 Å
• b: 13.205 ± 0.002 Å
• c: 36.708 ± 0.007 Å
• α: 90°
• β: 90.346 ± 0.003°
• γ: 90°
• Cell volume: 7787 ± 2 ų
• Cell temperature: 158 ± 2 K
• Ambient diffraction temperature: 158 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0486
• Residual factor for significantly intense reflections: 0.0392
• Weighted residual factors for significantly intense reflections: 0.0769
• Weighted residual factors for all reflections included in the refinement: 0.0813
• Goodness-of-fit parameter for all reflections included in the refinement: 1.114
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No