Information card for entry 4312551

Structure parameters

• Formula: C52 H62 Cl4 O9 P4 Pd2
• Calculated formula: C52 H42 Cl4 O9 P4 Pd2
• Title of publication: Enolphosphato-Phosphines: A New Class of P,O Ligands
• Authors of publication: Xavier Morise; Pierre Braunstein; Richard Welter
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7752 - 7765
• a: 24.9753 ± 0.0004 Å
• b: 9.8367 ± 0.0003 Å
• c: 23.6794 ± 0.0004 Å
• α: 90 ± 0.001°
• β: 96.923 ± 0.003°
• γ: 90 ± 0.001°
• Cell volume: 5775 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0636
• Residual factor for significantly intense reflections: 0.0501
• Weighted residual factors for significantly intense reflections: 0.1599
• Weighted residual factors for all reflections included in the refinement: 0.1742
• Goodness-of-fit parameter for all reflections included in the refinement: 1.288
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No