Information card for entry 4312552

Structure parameters

• Formula: C33 H38 F6 N O4 P3 Pd
• Calculated formula: C33 H38 F6 N O4 P3 Pd
• Title of publication: Enolphosphato-Phosphines: A New Class of P,O Ligands
• Authors of publication: Xavier Morise; Pierre Braunstein; Richard Welter
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7752 - 7765
• a: 10.3847 ± 0.0005 Å
• b: 21.2069 ± 0.0005 Å
• c: 16.9638 ± 0.0005 Å
• α: 90 ± 0.001°
• β: 100.346 ± 0.005°
• γ: 90 ± 0.001°
• Cell volume: 3675.2 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0874
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.1233
• Weighted residual factors for all reflections included in the refinement: 0.1593
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No