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Information card for entry 4313072
Preview
Coordinates | 4313072.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H39 Cl2 N P2 V |
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Calculated formula | C28 H39 Cl2 N P2 V |
SMILES | [V](Cl)(Cl)([P](C)(C)c1ccccc1)([P](C)(C)c1ccccc1)=Nc1c(cccc1C(C)C)C(C)C |
Title of publication | Synthesis and Crystal Structure of Unprecedented Phosphine Adducts of d1-Aryl Imido-Vanadium(IV) Complexes |
Authors of publication | Christian Lorber; Robert Choukroun; Bruno Donnadieu |
Journal of publication | Inorganic Chemistry |
Year of publication | 2003 |
Journal volume | 42 |
Pages of publication | 673 - 675 |
a | 12.09 ± 0.002 Å |
b | 16.489 ± 0.003 Å |
c | 29.815 ± 0.006 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5943.7 ± 1.9 Å3 |
Cell temperature | 180 ± 2 K |
Ambient diffraction temperature | 180 ± 2 K |
Number of distinct elements | 6 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0938 |
Residual factor for significantly intense reflections | 0.0817 |
Weighted residual factors for significantly intense reflections | 0.1323 |
Weighted residual factors for all reflections included in the refinement | 0.1378 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.256 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4313072.html
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