Information card for entry 4313073

Structure parameters

• Formula: C44 H86 Cl8 N2 P6 V2
• Calculated formula: C44 H86 Cl8 N2 P6 V2
• Title of publication: Synthesis and Crystal Structure of Unprecedented Phosphine Adducts of d1-Aryl Imido-Vanadium(IV) Complexes
• Authors of publication: Christian Lorber; Robert Choukroun; Bruno Donnadieu
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 673 - 675
• a: 10.769 ± 0.005 Å
• b: 15.902 ± 0.005 Å
• c: 18.413 ± 0.005 Å
• α: 90 ± 0.005°
• β: 90.66 ± 0.005°
• γ: 90 ± 0.005°
• Cell volume: 3153 ± 2 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0836
• Residual factor for significantly intense reflections: 0.0686
• Weighted residual factors for significantly intense reflections: 0.1307
• Weighted residual factors for all reflections included in the refinement: 0.1394
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No