Information card for entry 4313142

Structure parameters

• Common name: FeCl[N(TMS)2]2(THF)
• Formula: C16 H44 Cl Fe N2 O Si4
• Calculated formula: C16 H44 Cl Fe N2 O Si4
• Title of publication: Iron-Arylimide Clusters [Fem(NAr)nCl4]2- (m,n= 2, 2; 3, 4; 4, 4) from a Ferric Amide Precursor: Synthesis, Characterization, and Comparison to Fe-S Chemistry
• Authors of publication: Jeremiah S. Duncan; Tamim M. Nazif; Atul K. Verma; Sonny C. Lee
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1211 - 1224
• a: 8.3297 ± 0.0004 Å
• b: 11.4333 ± 0.0006 Å
• c: 15.7784 ± 0.0008 Å
• α: 105.188 ± 0.002°
• β: 92.64 ± 0.002°
• γ: 109.323 ± 0.002°
• Cell volume: 1353.88 ± 0.12 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0602
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for all reflections: 0.099
• Weighted residual factors for significantly intense reflections: 0.0901
• Goodness-of-fit parameter for all reflections: 1.065
• Goodness-of-fit parameter for significantly intense reflections: 1.122
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No