Information card for entry 4313143

Structure parameters

• Common name: [Fe2(mu-Cl)3(THF)6]2[Fe3(mu-NPh)4Cl4].THF
• Formula: C76 H124 Cl10 Fe7 N4 O13
• Calculated formula: C76 H108 Cl10 Fe7 N4 O13
• Title of publication: Iron-Arylimide Clusters [Fem(NAr)nCl4]2- (m,n= 2, 2; 3, 4; 4, 4) from a Ferric Amide Precursor: Synthesis, Characterization, and Comparison to Fe-S Chemistry
• Authors of publication: Jeremiah S. Duncan; Tamim M. Nazif; Atul K. Verma; Sonny C. Lee
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1211 - 1224
• a: 13.4941 ± 0.0007 Å
• b: 14.7117 ± 0.0006 Å
• c: 23.6266 ± 0.0013 Å
• α: 83.721 ± 0.002°
• β: 88.776 ± 0.002°
• γ: 87.477 ± 0.003°
• Cell volume: 4657.1 ± 0.4 ų
• Cell temperature: 175 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1668
• Residual factor for significantly intense reflections: 0.0679
• Weighted residual factors for all reflections: 0.1697
• Weighted residual factors for significantly intense reflections: 0.1338
• Goodness-of-fit parameter for all reflections: 1.029
• Goodness-of-fit parameter for significantly intense reflections: 1.204
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No