Information card for entry 4313278

Structure parameters

• Common name: holeb06
• Chemical name: (2,4-bis(2,6-diisopropylphenylimido)pentyl nickel bis(mu-chloro) lithium etherate
• Formula: C37 H49 Cl2 Li N2 Ni O2
• Calculated formula: C37 H49 Cl2 Li N2 Ni O2
• Title of publication: Nickel Complexes of a Bulky β-Diketiminate Ligand
• Authors of publication: Nathan A. Eckert; Emily M. Bones; Rene J. Lachicotte; Patrick L. Holland
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 1720 - 1725
• a: 19.708 ± 0.002 Å
• b: 9.7979 ± 0.0011 Å
• c: 21.389 ± 0.002 Å
• α: 90°
• β: 109.993 ± 0.002°
• γ: 90°
• Cell volume: 3881.2 ± 0.7 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1173
• Residual factor for significantly intense reflections: 0.0853
• Weighted residual factors for significantly intense reflections: 0.2168
• Weighted residual factors for all reflections included in the refinement: 0.238
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No