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Information card for entry 4313279
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Coordinates | 4313279.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | holne30 |
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Chemical name | (2,4-bis(2,6-diisopropylphenyl)imido)pentyl bis(trimethylsilyl)amido nickel(ii) |
Formula | C35 H59 N3 Ni Si2 |
Calculated formula | C35 H59 N3 Ni Si2 |
SMILES | [Ni]1(N(C(=CC(=[N]1c1c(cccc1C(C)C)C(C)C)C)C)c1c(cccc1C(C)C)C(C)C)N([Si](C)(C)C)[Si](C)(C)C |
Title of publication | Nickel Complexes of a Bulky β-Diketiminate Ligand |
Authors of publication | Nathan A. Eckert; Emily M. Bones; Rene J. Lachicotte; Patrick L. Holland |
Journal of publication | Inorganic Chemistry |
Year of publication | 2003 |
Journal volume | 42 |
Pages of publication | 1720 - 1725 |
a | 9.153 ± 0.0005 Å |
b | 20.2569 ± 0.001 Å |
c | 20.197 ± 0.001 Å |
α | 90° |
β | 90.785 ± 0.001° |
γ | 90° |
Cell volume | 3744.4 ± 0.3 Å3 |
Cell temperature | 193 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0871 |
Residual factor for significantly intense reflections | 0.0643 |
Weighted residual factors for significantly intense reflections | 0.1244 |
Weighted residual factors for all reflections included in the refinement | 0.1329 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.135 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4313279.html
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