Information card for entry 4313841

Structure parameters

• Formula: C40 H95 Li3 N9 O4 P3
• Calculated formula: C40 H95 Li3 N9 O4 P3
• Title of publication: Lithiation of Tris(alkyl- and arylamido)orthophosphates EP[N(H)R]3 (E = O, S, Se): Imido Substituent Effects and PE Bond Cleavage
• Authors of publication: Tristram Chivers; Mark Krahn; Gabriele Schatte; Masood Parvez
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 3994 - 4005
• a: 20.94 ± 0.003 Å
• b: 19.282 ± 0.003 Å
• c: 27.461 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 11088 ± 3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0839
• Residual factor for significantly intense reflections: 0.0439
• Weighted residual factors for significantly intense reflections: 0.1101
• Weighted residual factors for all reflections included in the refinement: 0.125
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No