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Information card for entry 4313842
Preview
Coordinates | 4313842.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C21 H54 Li2 N7 P S |
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Calculated formula | C21 H54 Li2 N7 P S |
SMILES | [S]12P(=[N](C(C)C)[Li]13[N](C)(C)CC[N]3(C)C)(N(C(C)C)[Li]12[N](C)(C)CC[N]1(C)C)NC(C)C |
Title of publication | Lithiation of Tris(alkyl- and arylamido)orthophosphates EP[N(H)R]3 (E = O, S, Se): Imido Substituent Effects and PE Bond Cleavage |
Authors of publication | Tristram Chivers; Mark Krahn; Gabriele Schatte; Masood Parvez |
Journal of publication | Inorganic Chemistry |
Year of publication | 2003 |
Journal volume | 42 |
Pages of publication | 3994 - 4005 |
a | 9.687 ± 0.0014 Å |
b | 12.3926 ± 0.0017 Å |
c | 14.357 ± 0.002 Å |
α | 86.402 ± 0.003° |
β | 75.281 ± 0.002° |
γ | 71.642 ± 0.003° |
Cell volume | 1581.8 ± 0.4 Å3 |
Cell temperature | 193 ± 2 K |
Ambient diffraction temperature | 193 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1027 |
Residual factor for significantly intense reflections | 0.0619 |
Weighted residual factors for significantly intense reflections | 0.1427 |
Weighted residual factors for all reflections included in the refinement | 0.1634 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.013 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4313842.html
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