Information card for entry 4313843

Structure parameters

• Formula: C32 H70 Li2 N6 O2 P2
• Calculated formula: C32 H73 Li2 N6 O2 P2
• Title of publication: Lithiation of Tris(alkyl- and arylamido)orthophosphates EP[N(H)R]3 (E = O, S, Se): Imido Substituent Effects and PE Bond Cleavage
• Authors of publication: Tristram Chivers; Mark Krahn; Gabriele Schatte; Masood Parvez
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 3994 - 4005
• a: 11.917 ± 0.006 Å
• b: 16.255 ± 0.008 Å
• c: 11.025 ± 0.005 Å
• α: 90°
• β: 108.76 ± 0.005°
• γ: 90°
• Cell volume: 2022.2 ± 1.7 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 8
• Hermann-Mauguin space group symbol: C 1 m 1
• Hall space group symbol: C -2y
• Residual factor for all reflections: 0.0915
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.0894
• Weighted residual factors for all reflections included in the refinement: 0.106
• Goodness-of-fit parameter for all reflections included in the refinement: 0.921
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No