Information card for entry 4314682

Structure parameters

• Formula: C53 H66 B2 F24 N P2 Rh
• Calculated formula: C53 H66 B2 F24 N P2 Rh
• Title of publication: Amine- and Dimeric Amino-Borane Complexes of the {Rh(PiPr3)2}+ Fragment and Their Relevance to the Transition-Metal-Mediated Dehydrocoupling of Amine-Boranes
• Authors of publication: Adrian B. Chaplin; Andrew S. Weller
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 1111 - 1121
• a: 12.4906 ± 0.0002 Å
• b: 13.4472 ± 0.0002 Å
• c: 19.3634 ± 0.0003 Å
• α: 77.0895 ± 0.0006°
• β: 86.5573 ± 0.0006°
• γ: 82.4775 ± 0.0005°
• Cell volume: 3141.25 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.05
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.1034
• Weighted residual factors for all reflections included in the refinement: 0.1087
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No