Crystallography Open Database

Information card for entry 4314683

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Coordinates	4314683.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H70 B3 F24 N2 P2 Rh
Calculated formula	C54 H70 B3 F24 N2 P2 Rh
Title of publication	Amine- and Dimeric Amino-Borane Complexes of the {Rh(PiPr3)2}+ Fragment and Their Relevance to the Transition-Metal-Mediated Dehydrocoupling of Amine-Boranes
Authors of publication	Adrian B. Chaplin; Andrew S. Weller
Journal of publication	Inorganic Chemistry
Year of publication	2010
Journal volume	49
Pages of publication	1111 - 1121
a	12.7699 ± 0.0001 Å
b	19.7241 ± 0.0001 Å
c	27.1519 ± 0.0002 Å
α	73.7772 ± 0.0002°
β	86.737 ± 0.0003°
γ	73.2126 ± 0.0003°
Cell volume	6284.62 ± 0.08 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0573
Residual factor for significantly intense reflections	0.0408
Weighted residual factors for significantly intense reflections	0.0952
Weighted residual factors for all reflections included in the refinement	0.1037
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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